NILU logo 
EBAS
Data Submission Manual
Login
Submit DataData ReportingTemplatesCategoryPersistent Organic PollutantsPOPs in air and aerosols    December 14, 2019
 
Minimize

Template for POPs in air and aerosols

This format should be used for submitting all relevant persistent organic pollutants (POPs) measured in gas phase and/or in aerosols.

Points to note:

  • Include information on filter and absorbent setup under meta data “medium”
  • Include information on how sample is treated in the lab under “sample preparation “. Use special setup with information on combination of Soxhlet+Hexane+13C+Silica -
  • Include information if been part of any relevant laboratory intercomparison in the QA measures.

Downloading template as text file

You could download the template and start to modify the text with your own metadata. Due to limitations of the online portal we could not provide files with the .nas file extension. So please download the text file and edit, and remember to use the .nas file-extension when you create your datafile: pops_air.txt

Validation and submission:

To validate the file, please use the EBAS Submission Tool

Flags commonly used with this format:

All the flags defined for EBAS can be used, and the data submitter is encourage to go through the list of all EBAS flags prior to submitting to ensure that appropriate flagging is done.
Flags are grouped in four categories: V (valid measurement), I (invalid measurement), M (missing measurement) or H (hidden and invalid measurements)..
Apply '000' for valid measurements without any annotations.
The most common flags for these measurements are:

Group 9: Missing flags

FlagValidityDescription
999MMissing measurement, unspecified reason

Group 7: Flags used when the value is unknown

FlagValidityDescription
781VValue below detection limit, data element contains detection limit

Group 6: Mechanical or instrumental problem

FlagValidityDescription
669IMoist or wet filter, invalid
668VMoist or wet filter, valid
666IFilter damaged, invalid
665VFilter damaged, valid
664IInstrument flow(s) too far off target value, considered invalid
663IToo high sampling flow, data considered invalid
662VToo high sampling flow, data considered valid
660VUnspecified sampling anomaly, considered valid
659IUnspecified sampling anomaly
658IToo small air volume
632VLid of polyurethane foam (PUF) sampler not closed
630VPOP concentration from the polyurethane foam (PUF) only

Group 5: Chemical problem

FlagValidityDescription
599IUnspecified contamination or local influence
591IAgricultural contamination, considered invalid
568IDust contamination, considered invalid
559VUnspecified contamination or local influence, but considered valid
558VDust contamination, but considered valid
549IImpure chemicals
540ISpectral interference in laboratory analysis
533IFilters mixed up; incorrect analysis
532VData less accurate than normal due to high field blank value
531VLow recovery, analysis inaccurate
530IInvalid due to too low or too high recovery

Group 4: Extreme or inconsistent values

FlagValidityDescription
460IContamination suspected

Group 1: Exception flags for accepted, irregular data

FlagValidityDescription
147VBelow theoretical detection limit or formal Q/A limit, but a value has been measured and reported and is considered valid

Template for Data Submission:

Clicking on a specific line in the example template will provide a detailed explanation and possible options for each of the metadata elements.

The example template given below contains the metadata fields that are commonly included when reporting data related to this specific template. Some of these metadata elements may not be relevant for your data reporting, like AIRS station ID for stations outside North America or the various QA measure data when there is no QA measure for the data. Such metadata elements could be let out. If you want to include additional metadata elements that are not given in the example template, there is a complete list here. In case of any doubt about such additional metadata, please consult the EBAS team!

94 1001
Enge, Ellen Katrin; Nizzetto, Pernilla Bohlin
NO01L, Norwegian Institute for Air Research, NILU, Atmosphere and Climate Department, Instituttveien 18, , 2007, Kjeller, Norway
Våler, Rita
CAMP EMEP NILU
1 1
2015 01 01 2016 01 15
7
days from file reference point
19
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
999.999999 99.99 9.999999 9.999 9.999999 9.9999 9.999999 9.9999 9.999999 9.9999 9.999999 9.99 9.999999 9.999 9.999999 9.999 9.999999 9.999 9.999999
end_time of measurement, days from the file reference point
HCB, pg/m3, Detection limit=0.01 pg/m3
numflag HCB, no unit
PCB_153, pg/m3, Detection limit=0.01 pg/m3
numflag PCB_153, no unit
PCB_180, pg/m3, Detection limit=0.01 pg/m3
numflag PCB_180, no unit
benzo_a_pyrene, ng/m3, Detection limit=0.001 ng/m3, Analytical measurement technique=GC/MS, Analytical instrument manufacturer=, Analytical instrument model=
numflag benzo_a_pyrene, no unit
pyrene, ng/m3, Detection limit=0.004 ng/m3, Analytical measurement technique=GC/MS, Analytical instrument manufacturer=, Analytical instrument model=
numflag pyrene, no unit
alpha_HCH, pg/m3, Detection limit=0.01 pg/m3
numflag alpha_HCH, no unit
gamma_HCH, pg/m3, Detection limit=0.01 pg/m3
numflag gamma_HCH, no unit
op_DDT, pg/m3, Detection limit=0.01 pg/m3
numflag op_DDT, no unit
pp_DDT, pg/m3, Detection limit=0.01 pg/m3
numflag pp_DDT, no unit

0
61
Data definition: EBAS_1.1
Set type code: TU
Timezone: UTC
File name: NO0002R.20150102063500.20160115000000.high_vol_sampler.pops.air+aerosol.1y.1d.NO01L_NILU_fppuf_01a.NO01L_NILU_O_2.lev2.nas
Startdate: 20150102063500
Revision date: 20160115000000
Version: 1
Version description: initial revision, manually inspected
Data level: 2
Period code: 1y
Resolution code: 1w
Sample duration: 1d
Station code: NO0002R
Platform code: NO0002S
Station name: Birkenes II
Station WDCA-ID: GAWANO__BIR
Station GAW-ID: BIR
Station GAW-Name: Birkenes Atmospheric Observatory
Station other IDs: 201(NILUDB)
Station land use: Forest
Station setting: Rural
Station GAW type: R
Station WMO region: 6
Station latitude: 58.38853
Station longitude: 8.252
Station altitude: 219.0m

Component: pops
Matrix: air+aerosol
Laboratory code: NO01L
Instrument type: high_vol_sampler
Instrument name: NILU_fppuf_01a
Instrument manufacturer: DIGITEL
Instrument model: DHA-80
Instrument serial number: 12345
Analytical laboratory code: NO01L
Analytical measurement technique: GC-HRMS
Analytical instrument name: NILU_GCMS
Analytical instrument manufacturer: Agilent
Analytical instrument model: 7000C
Method ref: NO01L_NILU_O_2
Standard method: SOP=EMEP_manual_v2014
Inlet type: Hat or hood
Inlet description: Downward facing
Flow rate: 140 l/min
Filter description: Whatman GF/C
Medium: Glass fiber+PUF+PUF
Sample preparation: Soxhlet+Hexane+13C+Silica
Blank correction: Not blank corrected
Humidity/temperature control: None
Humidity/temperature control description: filter kept at ambient conditions together with sampling head
Detection limit:
Detection limit expl.: Determined by taking 3 times standard deviation of ensemble of field blanks
Zero/negative values code: Zero/negative possible
Zero/negative values: Zero/negative values reported as measured if within detection limit, flagged with 147
QA1 measure ID: AMAP/EMEP/NCP_2010
QA1 date: 20100701
QA1 document URL: "http://www.nilu.no/projects/ccc/reports/cccr7-2011.pdf"

Originator: Enge, Ellen Katrin, eke@nilu.no, Norwegian Institute for Air Research, NILU, Environmental Chemistry Department, Instituttveien 18, , 2007, Kjeller, Norway
Originator: Nizzetto, Pernilla Bohlin, pbn@nilu.no, Norwegian Institute for Air Research, NILU, Environmental Chemistry Department, Instituttveien 18, , 2007, Kjeller, Norway

Submitter: Våler, Rita, rlv@nilu.no, Norwegian Institute for Air Research, NILU, Monitoring and Instrumentation Technology Department, Instituttveien 18, , 2007, Kjeller, Norway
Comment:
starttime endtime HCB flag_HCB PCB-153 flag_PCB-153 PCB-180 flag_PCB-180 C20H12 flag_C20H12 C16H10 flag_C16H10 alpha-HCH flag_alpha-HCH gamma-HCH flag_gamma-HCH op-DDT flag_op-DDT pp-DDT flag_pp-DDT
1.274306 2.272222 63.91 0.000000 0.136 0.000000 0.0248 0.000000 0.0179 0.000000 0.3120 0.000000 3.26 0.000000 0.837 0.000000 0.155 0.000000 0.123 0.000000
8.274306 9.272222 12.15 0.000000 0.042 0.000000 0.0113 0.000000 0.0112 0.000000 0.1276 0.000000 1.13 0.000000 0.345 0.000000 0.015 0.000000 0.015 0.000000


Version Information:

Last Change: 2019-07-24 12:25:40 UTC

  • linked list of valid parameters to component description

 Copyright 2009 by DotNetNuke Corporation   Terms Of Use  Privacy Statement